ketone-bisulfite product recrystallization. The solvent reduces mechanical loses, may make it easier to use the sep funnel - larger difference in specific gravities, lower would use a satured sodium bisulfite solution then add enough alcohol to make the solution more soluble in the nonpolar solvent...

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View CHM2210L_Formal_Report_Lab_part 8.docx from CHM 2210L at Miami Dade College, Miami. Post Lab Question: Solubility 1) According to your results, list the solids tested in order of increasing Purification (recrystallization if solid or distillation if liquid): (minutes to hours) Analysis (mp, spectroscopy, yield) (< I hr) The solvent in a traditional synthesis, as mentioned before, is usually a petroleum-based solvent, such as toluene, or a halogenated organic solvent, such as dichloromethane.

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